If it's a one-on-one fight Gojo probably wins, but if Makima's allowed to use all the resources Public Safety and the Japanese government has, things might get pretty ugly depending on how willing either of them are about civilian casualties.
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Power wise... honestly, I'm not sure who wins, at least when it comes to canon Makima. While she's not helpless on her own, most of her fighting potential comes from other people, which depends on what exactly she has available to her.